Analytical Instrumentation
Shimadzu GC2010 with Headspace HS-20NX
Technical data
Injector: max. temperature 450°C
Detector FID: max. temperature 450°C
(Hydogen flame ionisation detector )
Column oven: +4°C – 450°C
Coumns:
for example.: Ultra 1 (non polare, 100% dimethylpolysiloxane, max. 350°C), Ultra 2 (5% phenyl 95% dimethylpolysiloxane, max. 350°C), other columns are possible
Carrier gas: Hydrogen (Hydrogen generator Nitrox UHP-40H)
Contact
Annette Ricken Tel.: 0211 81-12874, e-mail:
Shimadzu GC 2014 with autosampler AOC-20i/s
Technical data
Injector: max. temperature 450°C
Detector FID: max. temperature 450°C
(Hydogen flame ionisation detector )
Column oven: +4°C – 450°C
Coumns:
for example.: Ultra 1 (non polare, 100% dimethylpolysiloxane, max. 350°C), Ultra 2 (5% phenyl 95% dimethylpolysiloxane, max. 350°C), other columns are possible
Carrier gas: Hydrogen (Hydrogen generator Nitrox UHP-40H)
Contact
Annette Ricken Tel.: 0211 81-12874, e-mail:
Bruker Kappa APEX-II Duo
Fully automatic Bruker Kappa APEX-II Duo single crystal X-ray diffractometer
- with dual wavelength system :
Cu-Kα (λ = 1.54178 Å) and Mo-Kα (λ = 0.71073 Å) sealed tube IµS sources
- high sensitivity 16 megapixel CCD area-detector and four-axis Kappa Goniostat
- measurements under reduced temperature are possible up to 90 K
The cooling system is an Oxford Cryostream 700 Series with liquid nitrogen cooling.
Contact:
Vera Vasylyeva-Shor Tel.: 0211-8112290 e-mail:
Takin Haj Hassani Sohi Tel.: 0211-8114390 e-mail:
Rigaku XtaLAB Synergy-S
The Rigaku XtaLAB Synergy-S is a dual microfocus X-ray diffractometer for fast and agile analysis of the 3D structure of single crystals.
Features:
Microfocus X-ray sources: Mo & Cu.
HyPix6000 photon hybrid detector.
Temperature control: 100 K - 400 K.
Optimal for small molecules.
Adjustable divergence slit option allows resolution of reflections from long unit cells (Cu only).
Powder X-ray diffractograms (PXRD) are also measurable (Cu & Mo).
Contact:
Vera Vasylyeva-Shor Tel.: 0211-8112290 e-mail:
Takin Haj Hassani Sohi Tel.: 0211-8114390 e-mail:
Bruker D2 Phaser
Measuring circle diameter:
141 mm
X-ray wavelength:
Cr / Co / Cu / Mo fused standard tube
X-ray power:
300 W, 30 kV, 10 mA max.
specimen movement:
Rotational movement
Contact:
Takin Haj Hassani Sohi Tel.: 0211/81-14390, e-mail:
Dr. Istvan Boldog Tel.: 0211/81-12292, e-mail:
Philipp Seifert Tel.: 0211/81-14390, e-mail:
Rigaku MiniFlex
Measurement geometry:
Reflection in θ/2θ. Sample moving, detector fixed. 2 ° - 140 °.
Radiation source:
Cu Kα 1.54182 Ǻ, power: 600 W 40kV 15 mA.
Contact:
Takin Haj Hassani Sohi Tel.: 0211/81-14390, e-mail:
Dr. Istvan Boldog Tel.: 0211/81-12292, e-mail:
Philipp Seifert Tel.: 0211/81-14390, e-mail:
3P Micro200
Connected gases:
Nitrogen (sample gas)
Helium
Measurement methods:
Simple BET measurement
Full isothermal
Special feature:
Two stations, decoupled from each other, at each of which one sample can be measured.
Simultaneous analysis of two samples and sample preparation of two samples.
Fully automatic measurement of specific surface area and pore size for meso- and micropores.
Small sample quantities can be measured
Short measuring times
Contact:
Linda Sonderman, Tel.: 0211/81-12596, e-mail:
Robert Oestreich, Tel.: 0211/81-13153, e-mail:
Annette Vollrath, Tel.: 0211/81-12292, e-mail:
Quantachrome Autosorb-6
Contact:
Marcus Fetzer Tel.: 0211/ 81 12292, e-mail:
Thi Hai Yen Beglau Tel.: 0211/ 81 12292, e-mail:
Belsorb Max II
Measurement methods:
- Simple BET isotherms
- Full isotherms
Connected gases:
Nitrogen (sample gas), argon, carbon dioxide, methane, hydrogen, helium.
Special features:
- Fully automatic measurement of specific surface area and pore size
- Simultaneous analysis of three samples and sample preparation
- Small sample amount can be measured
- Measurements at different temperatures are possible
- Short measuring times
Contact:
Linda Sonderman, Tel.: 0211/81-12596, e-mail:
Robert Oestreich, Tel.: 0211/81-13153, e-mail:
Annette Vollrath, Tel.: 0211/81-12292, e-mail:
QUANTACHrOME Autosorb-iQ-MP
Connected gases:
Nitrogen (sample gas)
Helium
Argon (sample gas)
Hydrogen (sample gas)
Carbon dioxide (sample gas)
Methane (sample gas)
Measuring methods:
Simple BET measurement
Full isothermal
Special feature:
Fully automatic measurement of the specific surface area and pore size
Simultaneous analysis of one sample and sample preparation of two samples
Very precise long-term measurements
Small sample quantities can be measured
Possibility of vapour sorption
High vacuum up to 1 x 10-7 mmHg
Measurements of isotherms of gases other than nitrogen (see connected gases).
Contact:
Linda Sondermann (Tel.: 0211/81-12596, e-mail:
Robert Oestreich (Tel.: 0211/81-13153, e-mail:
Nova
QUANTACHROME Nova 4200e S/N.
Connected gases:
Nitrogen (sample gas)
Helium
Measurement methods:
Simple BET measurement
Full isothermal
Special feature:
Fully automatic measurement of specific surface area and pore size.
Short measuring times
Up to 3 samples can be measured simultaneously
Small sample quantities can be measured
Contact:
Linda Sondermann Tel.: 0211/81-12596, e-mail:
Robert Oestreich Tel.: 0211/81-13153, e-mail:
Hanibal Othman Tel.: 0211/81-12874, e-mail:
RUBOTHERM IsoSORB STATIC (G-HP).
Connected gases:
Nitrogen (sample gas)
Carbon dioxide (sample gas)
Measurement methods:
Gravimetric sorption measurements
Special feature:
Automatic gravimetric high-pressure sorption measurements
Sample quantity: 100 mg - 10 g
Sample temperatures: -196°C up to 400°C
Contact:
Dustin Jorden (Tel.: 0211/81-13153, e-mail: )
Quantachrome Vstar
Volumetric vapour sorption device
Sample vapours:
Water, ethanol, benzene, cyclohexane, n-hexane and many more.
Measurement methods:
Volumetric measurements by p0-determination with helium
Measurements at various temperatures possible:
Temperature constancy guaranteed by circulating thermostat (operated with a water/ethylene glycol mixture). z. E.G. 20, 40, 60 °C
Special features:
Simultaneous measurement of up to 4 samples
High measuring accuracy with small sample quantities
Calculation of heat of adsorption or IAST selectivities (Ideal Adsorbed Spolution Theory) from the recorded isotherms
Contact:
Tim Müller Tel.: 0211/81-12874, e-mail: